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Beilstein J. Org. Chem. 2013, 9, 2194–2201, doi:10.3762/bjoc.9.258
Graphical Abstract
Figure 1: Several natural occurring anthracycline antibiotics.
Scheme 1: Total synthesis of daunomycinone 6 according to Hansen.
Scheme 2: Synthesis of simplified anthracycline derivatives.
Scheme 3: Retrosynthetic analysis of anthracycline aglycone mimics. Si: any silyl group.
Scheme 4: Synthetic route for the synthesis of various dialkynes 16. aSi: TMS, SiMe2Bn (2.0 equiv); Si: SiMe2...
Scheme 5: Silyl ether synthesis and domino carbopalladation reaction. R,R (Glc): isopropylidene. R,R (Gal): b...
Scheme 6: Derivatisation of anthracycline derivatives. aR,R (Glc): isopropylidene. R,R (Gal): benzylidene. Re...